phenohuntergarcia
Active Member
Here’s a Dry, Full Spectrum, Crystalline Extract that I made from Psilocybe mushrooms. No tek was followed. It’s my own method.
I analyzed it using HPLC with an iHILIC Classic Column then again with an iHILIC Fusion Column.
The Standard References used to detect active compounds were:
![5BF87181-B20D-4D04-8CF2-88E88F9CC201.jpeg](/data/attachments/4315/4315774-b7bf4e8923599b968de766b6c20aa078.jpg)
Potency was 2.38% active. Which is even higher than
Psilocybe azurescens (the strongest species in the Psilocybe genus).
![4ECCA294-52B1-439B-9276-9672223B4C8C.jpeg](/data/attachments/4315/4315775-22c1c64d5eddf00728cfda5e2b18861f.jpg)
![A16C4D01-EC99-4578-BF88-87BA414E657E.jpeg](/data/attachments/4315/4315783-a5b59a7d66c8dd3aad1f830c101c35b1.jpg)
The numbered peaks are the Standard References.
The un-numbered peaks are the Closely Related Compounds (MAOI’s).
Classic iHILIC Columns are used to analyze hydrophilic compounds![1DA775AF-A694-4CFF-995E-5CF5F05F9098.jpeg](/data/attachments/4315/4315776-bb99e22a639a56dbfd9fffb45726892a.jpg)
iHILIC Fusion Columns are used to detect both hydrophilic and hydrophobic compounds. I ran both columns just to verify the results.
![93305A3B-1836-4C12-9E5C-C72B8E39B09E.jpeg](/data/attachments/4315/4315777-7dc5c4cf383b3113fe712dd79270c6d1.jpg)
I analyzed it using HPLC with an iHILIC Classic Column then again with an iHILIC Fusion Column.
The Standard References used to detect active compounds were:
- Psilocybin
- Psilocin
- Norpsilocin
- Baeocystin
- Norbaeocystin
![5BF87181-B20D-4D04-8CF2-88E88F9CC201.jpeg](/data/attachments/4315/4315774-b7bf4e8923599b968de766b6c20aa078.jpg)
Potency was 2.38% active. Which is even higher than
Psilocybe azurescens (the strongest species in the Psilocybe genus).
![4ECCA294-52B1-439B-9276-9672223B4C8C.jpeg](/data/attachments/4315/4315775-22c1c64d5eddf00728cfda5e2b18861f.jpg)
![A16C4D01-EC99-4578-BF88-87BA414E657E.jpeg](/data/attachments/4315/4315783-a5b59a7d66c8dd3aad1f830c101c35b1.jpg)
The numbered peaks are the Standard References.
The un-numbered peaks are the Closely Related Compounds (MAOI’s).
Classic iHILIC Columns are used to analyze hydrophilic compounds
![1DA775AF-A694-4CFF-995E-5CF5F05F9098.jpeg](/data/attachments/4315/4315776-bb99e22a639a56dbfd9fffb45726892a.jpg)
iHILIC Fusion Columns are used to detect both hydrophilic and hydrophobic compounds. I ran both columns just to verify the results.
![93305A3B-1836-4C12-9E5C-C72B8E39B09E.jpeg](/data/attachments/4315/4315777-7dc5c4cf383b3113fe712dd79270c6d1.jpg)