What did you accomplish today?

manfredo

Well-Known Member
Does anything make it past the 25 bag when making bubble?
You have to shake it...It's all in the wrist! Did you make a work bucket drilled with holes to put your bags into?

Yeah teh 25's tricky
Baked the pie and assembled the lasagna

View attachment 4884400


View attachment 4884406
That looks delicious!! And it's a cold night here and now I want pasta!!

My grandma use to make lasagna with zucchini squash instead of the noodles sometimes...in the summer when there was an abundance of them...It was tasty!!
 

Mohican

Well-Known Member
Have fun!

FirstRunWM 02-06-14.png

FirstDrain 02-06-14.png

How many bags are you using?

Cut the bottom of the bucket off a third of the way up for each bag and stack those on top of an intact bucket.

220
190
120
73
45
25
Bucket​

All that remains in the bucket is some amazing smelling ice water, which I give to my blueberries.

I run the batch repeatedly until I don't get any resin.

73:

First73MicronMacro1 02-06-14.png

First73MicronMacro 02-06-14.png


Cheers,
Mo
 

manfredo

Well-Known Member
I have two buckets, I was going to use one for the work bag, then dump it into the second bucket with the smaller bags.
Here's how I do it.

I have my mixing buckets...regular 5 g buckets and I'll put about a gallon bags worth of frozen trim/smalls in the bucket, with a few inches of ice above and below it, then fill it with water above the ice and let it soak 15 minutes to saturate everything, with a few light stirrings. I usually have 3-4 buckets going.

Then I have another 5 gal. bucket with lots of big holes drilled in it. About 3/4" holes all over the sides and bottom, then I stack my bags in here. I only use the 36, 72, 90....those are the good ones. and I save 120 for food. I let the 25 go right down the drain!

So I have a total of 5 bags stacked...the 36,72,90, 120, and your work bag on top.

So now the material has been soaking for 15-20 minutes in ice water...you can mix it with the paint stirrer...gently, just for a few minutes the first time. The first run is usually the best stuff but you can keep re- running it until you stop getting hash...Usually at least 3-4 times, but I have gone 5-6 before. Then pour it through your bags. A laundry sink works great!! If you have more buckets, dump them through the screens.

THEN, you can pull your bags and collect the hash. You scrape it off gthe bottom with a plastic card then squeeze out the excess moisture. You can gte it to collect by bouncing the bag up and down quickly. Kinsd of a snapping motion gets it to gel together. Then I just use a towel and step on it inside a screen, then put it on a [piece of cardboard to dry...the cardboard helps pull the moisture out.

You'll be able to sample some while you work, but it'll be better tomorrow after drying some more. Then yo can press it, or chop it up, or whatever you want.

It is a lot of work and I always have a sore back the next day pouring all those buckets full of ice water and shaking the bags, etc. but I usually wind up with an ounce of full melt hash out of trim that would have been thrown away.

You'll gte better at it as time goes by, like everything.

Then I clean my bags good after by soaking them in a vinegar and dishsoap solution then wash them in the washing machine. I have the Bubble Bag Dude brand and they have been used 15+ times and still in good shape.

Have fun with it...Great sleep med!
 

manfredo

Well-Known Member
Damn I feel defeated.

Out of the 2 rotovapors I ordered, neither is happening. After getting the damaged one yesterday I checked tracking on the new one that was supposed to be delivered today. Well it hasn't been shipped, just a label created. Well after complaining I got a refund and told it was lost in shipping, which is a lie, but whatever.

In the meanwhile I have purchased everything else from a vacuum aspirator to Buchner funnel to syringes for this project....Damn!!

But I am a strong believer in fate, so maybe there's a reason...And the reason is I am going to start with basics, and get a cheap, basic vacuum distillation setup and go from there, just like they would in college! But I am still bummed!
 

Singlemalt

Well-Known Member
Damn I feel defeated.

Out of the 2 rotovapors I ordered, neither is happening. After getting the damaged one yesterday I checked tracking on the new one that was supposed to be delivered today. Well it hasn't been shipped, just a label created. Well after complaining I got a refund and told it was lost in shipping, which is a lie, but whatever.

In the meanwhile I have purchased everything else from a vacuum aspirator to Buchner funnel to syringes for this project....Damn!!

But I am a strong believer in fate, so maybe there's a reason...And the reason is I am going to start with basics, and get a cheap, basic vacuum distillation setup and go from there, just like they would in college! But I am still bummed!
You're in good shape and will find that you can do a lot with this, as you get familiar you'll start improvising. In labs, you learn how important the basics are
 

Singlemalt

Well-Known Member
Damn I feel defeated.

Out of the 2 rotovapors I ordered, neither is happening. After getting the damaged one yesterday I checked tracking on the new one that was supposed to be delivered today. Well it hasn't been shipped, just a label created. Well after complaining I got a refund and told it was lost in shipping, which is a lie, but whatever.

In the meanwhile I have purchased everything else from a vacuum aspirator to Buchner funnel to syringes for this project....Damn!!

But I am a strong believer in fate, so maybe there's a reason...And the reason is I am going to start with basics, and get a cheap, basic vacuum distillation setup and go from there, just like they would in college! But I am still bummed!
Either I haven't seen or forgot to ask; do have any separatory funnels? Extremely handy to have
sep funnel.jpg
 

manfredo

Well-Known Member
Either I haven't seen or forgot to ask; do have any separatory funnels? Extremely handy to have
View attachment 4884894
I am going to order a distillation set today, but not really sure which one yet. Maybe something like this... Is steam distillation something that is done with cannabis? They have the separator mislabeled in this diagram

1619103229944.png


1619103229944.png
 

Singlemalt

Well-Known Member
I am going to order a distillation set today, but not really sure which one yet. Maybe something like this... Is steam distillation something that is done with cannabis? They have the separator mislabeled in this diagram

View attachment 4884911


View attachment 4884911
steam distillation is used in CBD and in terpene extractions
edit: but it's not thatefficient in CBD, plus if not careful controlling temp it can damage CBD. It's a common process for extracting plant oils like in the perfume industry
 

raratt

Well-Known Member
Have fun!

View attachment 4884568

View attachment 4884560

How many bags are you using?

Cut the bottom of the bucket off a third of the way up for each bag and stack those on top of an intact bucket.

220
190
120
73
45
25
Bucket​

All that remains in the bucket is some amazing smelling ice water, which I give to my blueberries.

I run the batch repeatedly until I don't get any resin.

73:

View attachment 4884570

View attachment 4884571


Cheers,
Mo
Have you ever used a 220 zipper bag in the machine? I've seen those before. I don't plan on getting a machine unless I get some donations for what I make to pay for it.
 
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